HuagongsheHuagongshe Chemistry Print Report · For research reference only
4'-Bromobiphenyl-4-sulfonyl chloride → HCID 22721817, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4'-Bromobiphenyl-4-sulfonyl chloride | HCID 2756845 | — |
| Reactant | HCID 22721904 | HCID 22721904 | — |
| Product | HCID 22721817 | HCID 22721817 | 90% |
Reaction Steps
Using an analogous procedure to that described in Example 89, 4-[4-(4-pyridyl)piperazin-1-ylcarbonyl]aniline was reacted with 4′-bromo-4-biphenylylsulphonyl chloride to give N-{4-[4-(4-pyridyl)piperazin-1-ylcarbonyl]phenyl}-4′-bromo-4-biphenylylsulphonamide hydrochloride salt in 90% yield, m.p. 201-205° C.;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06225309B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-ac48079824894d8b9493eab391ad2d3b |
| Source note | uspto-grants-2001_05 |