HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → 4-Bromo-5-methoxy-2-(trifluoromethyl)pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 22000199 | HCID 22000199 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 4-Bromo-5-methoxy-2-(trifluoromethyl)pyridine | HCID 22000172 | — |
Reaction Steps
Prepared from bromine (0.21 ml, 4 mmol) and a solution of 3-methoxy-6-trifluoromethyl-2-trimethylstannylpyridine (0.7 g, 2.0 mmol) in dichloromethane (10 ml) according to the method of Description 42 to afford 4-bromo-3-methoxy-6-trifluoromethylpyridine as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06225320B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-4fdbbc75c7944e7ba613954fef208938 |
| Source note | uspto-grants-2001_05 |