HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylamine → HCID 178420472, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylamine | HCID 7582 | — |
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | HCID 178427483 | HCID 178427483 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178420472 | HCID 178420472 | 88.1% |
Reaction Steps
A solution of dicyclohexylamine (0.54 g) in AcOEt (1 ml) was added to a solution of N-(2-carboxymethyl-2,5,7,8-tetramethylchroman-6-sulfonyl)benzamidine (1.27 g) in AcOEt (11 ml) at room temperature. Diisopropyl ether (10 ml) was added and the mixture was stirred at room temperature to give N-(2-carboxymethyl-2,5,7,8-tetramethylchroman-6-sulfonyl)benzamidine dicyclohexylamine salt as a solid (1.59 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06225480B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-441e4b1b9c6a49ea94c10e65aa399b47 |
| Source note | uspto-grants-2001_05 |