HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylamine → HCID 178420471, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylamine | HCID 7582 | — |
| Reactant | HCID 178421531 | HCID 178421531 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178420471 | HCID 178420471 | 85.9% |
Reaction Steps
A solution of dicyclohexylamine (0.22 g) in AcOEt (1 ml) was added to a solution of N-(2-carboxymethyl-3,4,7,8,9,10-hexahydro-2,5-dimethyl-2H-naphtho[2,1-e]pyran-6-sulfonyl)benzamidine (0.55 g) in AcOEt (4 ml) and the mixture was stirred at room temperature to give N-(2-carboxymethyl-3,4,7,8,9,10-hexahydro-2,5-dimethyl-2H-naphtho[2,1-e]pyran-6-sulfonyl)benzamidine dicyclohexylamine salt as a solid (0.66 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06225480B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-7b6e951f49d24f75a722ac46a833be29 |
| Source note | uspto-grants-2001_05 |