HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-chloropropane → HCID 22644706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Reactant | HCID 54394859 | HCID 54394859 | — |
| Product | HCID 22644706 | HCID 22644706 | 75% |
Reaction Steps
According to the procedure of Example 5, 1.00 g (2.95 mmol) 2-(4but-2-ynyloxy-benzenesulfonylamino)-3-methyl-butyric acid methyl ester and 0.88 mL (8.849 mmol) of 1-bromo-3-chloropropane provided 0.92 g of methyl2-[{[4-(2-butynyloxy)penyl]sulfonyl}(3-chloropropyl)amino]-3-methylbutanoate as a white solid. Electrospray Mass Spec 416.2 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06225311B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-01be94561fe24fa5aff3f19723026f4b |
| Source note | uspto-grants-2001_05 |