HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 15458808, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 1-Methyl-6-nitro-1H-indole | HCID 10607359 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 15458808 | HCID 15458808 | 96% |
Reaction Steps
A stirred solution of 1-methyl-6-nitro-1H-indole in diethyl ether (Et2O) (5 mL) was cooled to 0° C., and treated with oxalyl chloride (0.15 mL, 1.7 mm). After stirring at room temperature overnight, solids were collected, washed with ether and dried to afford (255 mg, 96%) (1-methyl-6-nitro-1H-indol-3-yl)-oxo-acetyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06228877B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-f33481816f434e8099713c881010763f |
| Source note | uspto-grants-2001_05 |