HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetone → HCID 21998742, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetone | HCID 11715 | — |
| Reactant | Methyl 6-methylnicotinate | HCID 231548 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21998742 | HCID 21998742 | — |
Reaction Steps
A solution of methyl 6-methylnicotinate (1.00 g, 6.60 mmol) and bromoacetone (1.00 g, 7.30 mmol) in acetone (3 mL) was refluxed overnight, cooled to room temperature, and decanted. The resulting solid was dried under vacuum to provide approximatelyl.47 g the desired product as a solid, which was used directly in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06228868B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-ccd3ac7abf5444f6b7100e00f04d69a9 |
| Source note | uspto-grants-2001_05 |