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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1976776Generated: October 31, 2026

Bromoacetone → HCID 21998742, compound

https://huagongshe.com/reaction/1976776

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBromoacetoneHCID 11715—
ReactantMethyl 6-methylnicotinateHCID 231548—
SolventAcetoneHCID 180—
ProductHCID 21998742HCID 21998742—

Reaction Steps

A solution of methyl 6-methylnicotinate (1.00 g, 6.60 mmol) and bromoacetone (1.00 g, 7.30 mmol) in acetone (3 mL) was refluxed overnight, cooled to room temperature, and decanted. The resulting solid was dried under vacuum to provide approximatelyl.47 g the desired product as a solid, which was used directly in the next step without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06228868B1
Source datasetuspto-grants-2001_05
ORD IDord-ccd3ac7abf5444f6b7100e00f04d69a9
Source noteuspto-grants-2001_05