HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-hydroxybenzoic acid → HCID 57193022, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-hydroxybenzoic acid | HCID 91821 | — |
| Reactant | 4-(2,6-Dichlorobenzoylamino)-L-phenylalanine methyl ester | HCID 23383933 | — |
| Product | HCID 57193022 | HCID 57193022 | 35% |
Reaction Steps
4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[(2-chloro4-hydroxyphenyl)carbonyl]-L-phenylalanine methyl ester was prepared in 35% yield from 4-[[(2,6-dichlorophenyl)carbonyl]amino]-L-phenylalanine methyl ester and 2-chloro-4-hydroxybenzoic acid using the general procedure described in example 3. HR MS: Obs. mass, 521.0433. Calcd. mass, 521.0438 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06229011B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-4d3f35f05489473cb5be402eaf52d223 |
| Source note | uspto-grants-2001_05 |