HRID1976995

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2735589

2-Bromo-6-methylbenzoic acid

C8H7BrO2

结构：COC(=O)[C@@H](N)Cc1ccc(NC(=O)c2c(Cl)cccc2Cl)cc1

HCID23383933

未命名化合物

PRODUCTS

生成物

结构：COC(=O)[C@H](Cc1ccc(NC(=O)c2c(Cl)cccc2Cl)cc1)NC(=O)c1c(C)cccc1Br

HCID53758850

未命名化合物

收率 64%

PROCEDURE

实验过程

4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[(2-bromo-6-methylphenyl)carbonyl]-L-phenylalanine methyl ester was prepared in 64% yield from 4-[[(2,6-dichlorophenyl)carbonyl]amino]-L-phenylalanine methyl ester and 2-bromo-6-methylbenzoic acid using the general procedure described in example 3. HR MS: Obs. mass, 563.0138. Calcd. mass, 563.0140 (M+H).