HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-6-methylbenzoic acid → 4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[(2-bromo-6-methylphenyl)carbonyl]-L-phenylalanine methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-6-methylbenzoic acid | HCID 2735589 | — |
| Reactant | 4-(2,6-Dichlorobenzoylamino)-L-phenylalanine methyl ester | HCID 23383933 | — |
| Product | 4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[(2-bromo-6-methylphenyl)carbonyl]-L-phenylalanine methyl ester | HCID 53758850 | 64% |
Reaction Steps
4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[(2-bromo-6-methylphenyl)carbonyl]-L-phenylalanine methyl ester was prepared in 64% yield from 4-[[(2,6-dichlorophenyl)carbonyl]amino]-L-phenylalanine methyl ester and 2-bromo-6-methylbenzoic acid using the general procedure described in example 3. HR MS: Obs. mass, 563.0138. Calcd. mass, 563.0140 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06229011B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-de1e3a1fcaa5424f9d6366fdd122164d |
| Source note | uspto-grants-2001_05 |