HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 15405497, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 1,3-Propanediol | HCID 10442 | — |
| Reactant | HCID 21997415 | HCID 21997415 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15405497 | HCID 15405497 | — |
Reaction Steps
1.0 g (3.2 mmol) of 4-cyano-5-formyl-1-(4-chloro-1-methyl-5-methylsulfonyl-3-pyrazolyl)pyrazole, 0.35 g (4.6 mmol) of 1,3-dihydroxypropane and 10 mg of p-toluenesulfonic acid in 40 ml of toluene are heated on a water separator for 3 hours. Work-up as in Example 1.3 gives the title compound in the form of colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06232271B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-6cb953e82eee4b90a4d1f3cf063de93e |
| Source note | uspto-grants-2001_05 |