HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 712932, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 70053962 | HCID 70053962 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 712932 | HCID 712932 | 99.7% |
Reaction Steps
To a solution of 4-(5-amino-1,3,4-thiadiazol-2-yl)benzoic acid methyl ester trifluoroacetic acid salt (8 g) in water was added 1N sodium hydroxide and the mixture was adjusted to pH 8. The precipitate was collected by filtration to give 4-(5-amino-1,3,4-thiadiazol-2-yl)benzoic acid (5.05 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06232290B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-46f2294dd12648d88ddd4544db7fcdd9 |
| Source note | uspto-grants-2001_05 |