HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenemethanamine, 3,4-dichloro- → HCID 18617109, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenemethanamine, 3,4-dichloro- | HCID 1608 | — |
| Reactant | Benzoyl chloride, 3-(chlorosulfonyl)- | HCID 77671 | — |
| Reactant | HCID 57282618 | HCID 57282618 | — |
| Product | HCID 18617109 | HCID 18617109 | 28% |
Reaction Steps
Starting material (17(c)) was prepared as follows. 3,4-Dichlorobenzylamine was coupled with 3-Chlorosulphonylbenzoyl chloride (analogously as for compound (15(a)) in Example 15) to give 3-(3,4-dichloro-benzylcarbamoyl)-benzene-sulfonyl-chloride (17(a)) in 28% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06232338B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-26b4fca42a4043e489458e0b951107fd |
| Source note | uspto-grants-2001_05 |