HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 532661, compound → 4-(tert-Butyldimethylsiloxy)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 532661 | HCID 532661 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 4-(tert-Butyldimethylsiloxy)phenol | HCID 597388 | 97% |
Reaction Steps
1-(Benzyloxy)-4-(tert-butyldimethylsilyloxy)benzene was dissolved in ethyl acetate (400 ml) and 5 g of palladium on active carbon (5%) were added. After hydrogenation, the catalyst was removed by filtration and the solvents were removed under vacuo, to yield 42 g of 4-(tert-butyldimethylsilyloxy)-phenol (97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06232430B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-35f7b3dc1a6b4e46a27f68465bd3f854 |
| Source note | uspto-grants-2001_05 |