Azide → HCID 178485599, compound

HRID 1977501Notes

Reaction equation

C1(S([C:10](=[CH:15][C:16]2[CH:21]=[C:20]([C:22]([CH3:25])([CH3:24])[CH3:23])[C:19]([OH:26])=[C:18]([C:27]([CH3:30])([CH3:29])[CH3:28])[CH:17]=2)[C:11]([NH:13][CH3:14])=[O:12])(=O)=O)C=CC=CC=1.[N-:31]=[N+:32]=[N-:33]>>[CH3:30][C:27]([C:18]1[CH:17]=[C:16]([C:15]2[NH:31][N:32]=[N:33][C:10]=2[C:11]([NH:13][CH3:14])=[O:12])[CH:21]=[C:20]([C:22]([CH3:23])([CH3:24])[CH3:25])[C:19]=1[OH:26])([CH3:28])[CH3:29]

Participants

Reactant 2

HCID 33558Azide

HCID 53679181HCID 53679181, compound

Product 1

HCID 178485599HCID 178485599, compound

Procedure

reacting 2-(benzenesulfonyl)-3-[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]-N-methylacrylamide with a metal azide to yield 4-[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]-N-methyl-3H-[1,2,3]triazole-5-carboxamide.

Sources & evidence

ORD record: ord-ac1dc9214b39419388de998618718f53
Source dataset: uspto-grants-2001_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06232471B1

Reaction notes

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