HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 135815270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Chloro(phenyl)acetyl chloride | HCID 102902 | — |
| Reactant | 4-Amino-1-methyl-3-propyl-1H-pyrazole-5-carboxamide | HCID 3338044 | — |
| Product | HCID 135815270 | HCID 135815270 | — |
Reaction Steps
2-chloro-2-phenylacetyl chloride (3.47 ml, 0.022 mol) was added dropwise to a solution of 4-amino-3-propyl-1-methyl-5-pyrazolecarboxamide (4 g, 0.022 mol) in acetic acid (30 ml) and the reaction stirred at reflux under a nitrogen atmosphere for 20 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235742B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-8966729b39cd4cf981735bdddac69518 |
| Source note | uspto-grants-2001_05 |