HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromobenzene → HCID 21993536, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromobenzene | HCID 7961 | — |
| Reactant | N-(3-Fluorophenyl)acetamide | HCID 9594 | — |
| Product | HCID 21993536 | HCID 21993536 | 21.2% |
Reaction Steps
Using 3-fluoroacetanilide (4.6 g) and bromobenzene (9.4 g), a reaction was made in the same manner as in 1) of Production Example 14. The subsequent purification by silica gel column chromatography (developing solvent, ethyl acetate:hexane=1:2) produced 3-fluoro-N-phenylacetanilide (1.46 g; yield, 21%) as a purple oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235730B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-6060048376854ac9acfdee574857f168 |
| Source note | uspto-grants-2001_05 |