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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1978019Generated: October 28, 2026

1-[2-(Acetylamino)ethyl]-6-methoxyindan → (s)-1-[2-(Acetylamino)ethyl]-6-methoxyindan

https://huagongshe.com/reaction/1978019

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-[2-(Acetylamino)ethyl]-6-methoxyindanHCID 15523939—
SolventChloroformHCID 6212—
Product(s)-1-[2-(Acetylamino)ethyl]-6-methoxyindanHCID 10988162—

Reaction Steps

By substantially the same procedure as in Working Example 65, 1-[2-(acetylamino)ethyl]-6-methoxyindan was subjected to optical resolution by means of a high performance liquid chromatography to give the above-titled compound (119 mg), m.p.93-94° C. [α]Hg365 +80.7° (c 0.3, CHCl3).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06235789B1
Source datasetuspto-grants-2001_05
ORD IDord-41d58bf37abb4a7bb7738de8cea8386d
Source noteuspto-grants-2001_05