HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-hydroxyadamantane-1-carboxylate → 1-Methoxycarbonyl-3-acryloyloxyadamantane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-hydroxyadamantane-1-carboxylate | HCID 144304 | — |
| Reactant | 1-Hydroxy-3-(acryloyloxymethyl)adamantane | HCID 21996783 | — |
| Product | 1-Methoxycarbonyl-3-acryloyloxyadamantane | HCID 21996778 | 87% |
Reaction Steps
The reaction was conducted in the same manner as the step of Example 36 (2) except that 1-methoxycarbonyl-3-hydroxyadamantane was used instead of the 1,3-dicarboxy-5-adamantanol, and, as a result, a 1-methoxycarbonyl-3-acryloyloxyadamantane (yield: 87%, white solid) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235851B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-c9786bc93c7743adb0418a5c12b41e1d |
| Source note | uspto-grants-2001_05 |