HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86195276, compound → HCID 21997027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86195276 | HCID 86195276 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 21997027 | HCID 21997027 | — |
Reaction Steps
A mixture of 2-[(n-butylsulfonyl)methyl)-3-(n-butylsulfonyl)-propanoic acid, ethyl ester (1.0 g, 3.0 mmol) in 6N hydrochloric acid ( 20 mL) is refluxed overnight. The mixture is transferred to distilled water and extracted with ethyl acetate. The combined organic extracts are concentrated in vacuo to yield the title compound as a clear, colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235928B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-8fb333f335fd4a3aa249652a3f1b0642 |
| Source note | uspto-grants-2001_05 |