HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexafluoroacetone → 1,1,1,3,3,3-Hexafluoro-2-propanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexafluoroacetone | HCID 12695 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 1,1,1,3,3,3-Hexafluoro-2-propanol | HCID 13529 | 90% |
Reaction Steps
Approximately 100cc of Pd/C catalyst is packed into a ½″ diameter pipe reactor. Approximately 1 g/min of the hexafluoroacetone and 500cc/min hydrogen gas is fed into the reactor at atmospheric pressure and 180° C. Hexafluoro-2-propanol is produced in greater than 90% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235950B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-c0a60bd35ca942bbbb3d589ef84535ae |
| Source note | uspto-grants-2001_05 |