HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1,1,3,3,3-Hexafluoro-2-propanol → 1,1,1,2,3,3,3-Heptafluoropropane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1,1,3,3,3-Hexafluoro-2-propanol | HCID 13529 | — |
| Reactant | Fluorine | HCID 24524 | — |
| Product | 1,1,1,2,3,3,3-Heptafluoropropane | HCID 67940 | 90% |
Reaction Steps
A vapor plug flow reactor ½″ diameter×3′ long Monel® pipe is fed with 1 g/min of the hexafluoro-2-propanol and 150 cc/min of elemental fluorine at ambient conditions to produce 1,1,1,2,3,3,3 heptafluoropropane in greater than 90% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235950B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-8091449eafa5418285f4ceb12e803ba3 |
| Source note | uspto-grants-2001_05 |