HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 9951648, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | HCID 131719100 | HCID 131719100 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 9951648 | HCID 9951648 | 64% |
Reaction Steps
This compound was synthesized from protected α-ketoester derived from Z—Leu—Abu—CO2Et and ethylamine in 64% yield by the procedure described in Example 1. Single spot on TlC, Rf=0.36 (CHCl3/CH3OH 50;1); mp 130-132° C. Anal. calcd. for C21H31N3O5:405.45; C, 62.20; H, 7.71; N, 10.36. Found: C, 61.92; H, 7.62; N, 10.31. NMR (CDCl3) ok. MS (FAB) m/e=406 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235929B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-c66d5a6de9be4469ac83e4b9749c1c60 |
| Source note | uspto-grants-2001_05 |