HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14235690, compound → HCID 131722576, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14235690 | HCID 14235690 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 131722576 | HCID 131722576 | 87% |
Reaction Steps
The t-butyl ester (10, 100 mg, 0.22 mmol) in trifluoroacetic acid (5 mL) was stirred in an ice bath for 30 minutes. Trifluoroacetic acid was removed under reduced pressure, the crude product was recrystallized from EtOAc/hexane to give 76.8 mg (0.19 mmol, 87% yield) of a pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235929B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-655ba1c6c24748afa650429612bd3e35 |
| Source note | uspto-grants-2001_05 |