HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → 1,7,13-Triazatridecane Trihydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Phenol | HCID 996 | — |
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | 7-Mesitylenesulfonyl-1,7,13-triazatridecane | HCID 10785355 | — |
| Product | 1,7,13-Triazatridecane Trihydrochloride | HCID 21996659 | — |
Reaction Steps
HBr (30% in HOAc, 26 mL), 42 (2.0 g, 5.42 mmol), and phenol (4.8 g, 51 mmol) in CHCl3 (40 mL) were reacted, and product was isolated by the method of 2 to give 0.97 (61%) of 24 as a white solid: NMR (D2O) δ 1.45 (m, 4 H), 1.70 (m, 8 H), 3.01 (m, 8 H). Anal. (C10H28Cl3N3) C, H, N.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235794B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-475f4d3908c14891b456e6e39552e687 |
| Source note | uspto-grants-2001_05 |