反应详情

HBr (30% in HOAc, 26 mL), 42 (2.0 g, 5.42 mmol), and phenol (4.8 g, 51 mmol) in CHCl3 (40 mL) were reacted, and product was isolated by the method of 2 to give 0.97 (61%) of 24 as a white solid: NMR (D2O) δ 1.45 (m, 4 H), 1.70 (m, 8 H), 3.01 (m, 8 H). Anal. (C10H28Cl3N3) C, H, N.

1. customproduct was isolated by the method of 2