Hydrogen Bromide → HCID 21996675, compound

Participants

Reaction Steps

HBr (30% in HOAc, 30 mL), 55 (1.48 g, 1.94 mmol), and phenol (5.2 g, 55 mmol) in CH2Cl2 (30 mL) were reacted, and product was isolated by the method of 2 to produce 480 mg (76%) of 25 as needles: NMR (D2O) δ 1.4-1.5 (quintet, 4 H), 1.7-1.8 (quintet, 8 H), 2.7 (s, 6 H), 3.05 (t, 8 H, J=7). Anal. (C12H32Cl3N3) C, H, N.

Provenance & Evidence