Hydrogen Bromide → HCID 21996660, compound

Participants

Reaction Steps

HBr (30% in HOAc, 20 mL), 56 (2.9 g, 3.67 mmol), and phenol (3.25 g, 34.5 mmol) in CHCl3 (27 mL) were reacted, and product was isolated by the method of 2 to give 1.0 g (77%) of 26 as white crystals: NMR (D2O) δ 1.28 (t, 6 H, J=7), 1.45 (m, 4 H), 1.73 (m, 8 H), 3.08 (m, 12 H). Anal. (C14H36Cl3N3) C, H, N.

Provenance & Evidence