HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 21996672, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Phenol | HCID 996 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 10581933 | HCID 10581933 | — |
| Product | HCID 21996672 | HCID 21996672 | 81% |
Reaction Steps
HBr (30% in HOAc, 195 mL), 79 (12.66 g, 12.1 mmol), and phenol (33.61 g, 0.357 mol) in CH2Cl2 (135 mL) were reacted, and product was isolated by the method of 2 to provide 4.50 g (81%) of 29 as white crystals: NMR (D2O) δ 1.28 (t, 6 H, J=7), 1.40-1.52 (m, 4 H), 1.66-1.80 (m, 12 H), 3.00-3.14 (m, 16 H). Anal. (C18H46Cl4N4).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235794B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-4bbb188d4a6340a6bfeb330dd360a0f8 |
| Source note | uspto-grants-2001_05 |