HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21994001, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21994196 | HCID 21994196 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21994001 | HCID 21994001 | — |
Reaction Steps
In 50 ml of methanol was dissolved 8.902 g of N-tert-butoxycarbonyl-[1-(3-phenylpropan-1-yl)piperidin-3-ylmethyl]amine, followed by addition of 10 ml of concentrated hydrochloric acid, and the mixture was stirred at room temperature for 3 hours. This reaction mixture was concentrated to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235731B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-846c857edee842d59a5b49c05b6946cb |
| Source note | uspto-grants-2001_05 |