Hydrochloric Acid → HCID 21994184, compound

Participants

Reaction Steps

To a solution of 15.021 g (39.368 mM) of N-[2-(tert-butyldimethylsilyloxymethyl)benzyl]phthalimide in 50 ml of methanol was added 5 ml of concentrated hydrochloric acid at room temperature and the mixture was stirred at the prevailing temperature for 10 minutes. This reaction mixture was poured in water-diethyl ether and the resulting precipitate was recovered, rinsed serially with water and diethyl ether, and dried to provide the title compound.

Provenance & Evidence