Hydrochloric Acid → HCID 21994199, compound

Participants

Reaction Steps

To a solution of 3.550 g (9.902 mM) of tert-butyl 4-(4-phenylpiperidinomethyl)piperidine-1-carboxylate in 30 ml of methanol was added 5 ml of concentrated hydrochloric acid and the mixture was stirred at room temperature for 3 hours. The solvent was then distilled off and the residue was crystallized from ethanol-diethyl ether to provide the title compound.

Provenance & Evidence