HRID1978391

反应详情

EQUATION

反应方程式

HRID 1978391 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

(E)-Ethyl 3-(4-nitrophenyl)acrylate (11.7 g, 52.9 mmol) in tetrahydrofuran (100 ml) was hydrogenated over 10% Palladium-Carbon (1.20 g) at atmospheric pressure. After removal of the catalyst, the filtrate was concentrated in vacuo to give ethyl 3-(4-aminophenyl)propionate as a yellow oil (9.66 g, 95%).

WORKUP

后处理

  1. customAfter removal of the catalyst
  2. concentrationthe filtrate was concentrated in vacuo