Hydrochloric Acid → HCID 21993757, compound

Participants

Reaction Steps

To a solution of 3.37 g (7.86 mM) of N-[2-(1-tert-butoxycarbonyl-4-piperidyl)ethyl]-5-thia-1,8b-diazaacenaphthylene-4-carboxamide in ethanol (100 ml) was added 12N-hydrochloric acid (3.2 ml, 39.3 mM) and the mixture was stirred at room temperature for 1 hour. The resulting crystals were collected by filtration and rinsed with small amounts of ethanol and ether to provide the title compound.

Provenance & Evidence