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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1978505Generated: October 30, 2026

Hydrochloric Acid → HCID 21993852, compound

https://huagongshe.com/reaction/1978505

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 21993692HCID 21993692—
SolventMethanolHCID 887—
ProductHCID 21993852HCID 21993852—

Reaction Steps

In 2 ml of methanol was dissolved 0.233 g of (E)-4-[2-[1-(3-phenylpropan-1-yl)piperidin-4-ylmethylthio]-vinyl]-5-thia-1,8b-diazaacenaphthylene, followed by addition of a stoichiometric excess of methanolic hydrochloric acid, and the mixture was stirred for 10 minutes. This reaction mixture was concentrated to provide the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06235731B1
Source datasetuspto-grants-2001_05
ORD IDord-a831a051a01640f390dfb8cfb7ccfce8
Source noteuspto-grants-2001_05