HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70247634, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 70246921 | HCID 70246921 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70247634 | HCID 70247634 | — |
Reaction Steps
In 2 ml of methanol was dissolved 0.217 g of (E)-N-[1-(3-phenylpropan-1-yl)piperidin-4-ylmethyl]-2-(5-thia-1,8b-diazaacenaphthylen-4-yl)vinylsulfonamide, followed by addition of a stoichiometric excess of methanolic hydrochloric acid, and the mixture was stirred for 10 minutes. This reaction mixture was concentrated to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06235731B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-52d9181115534013823e5f6a9622d8f2 |
| Source note | uspto-grants-2001_05 |