Hydrochloric Acid → HCID 21993654, compound

Participants

Reaction Steps

To a solution of 1.16 g (2.51 mmol.) of N-[4-(4-benzoylpiperazin-1-yl)butan-1-yl]-5-thia-1,8b-diazaacenaphthylene-4-carboxamide in ethanol was added, at room temperature, 1 ml (12 mmol.) of 12N hydrochloric acid. The mixture was stirred for several minutes. The resulting crystals were collected by filtration and washed with ethanol and diethyl ether to give the object compound as orange crystals. The yield was 0.918 g (69%).

Provenance & Evidence