Hydrochloric Acid → HCID 21994149, compound

Participants

Reaction Steps

To a solution of 329.7 mg (0.65 mmol.) of N-[1-[3-(4-ethoxycarbonylphenoxy)propan-1-yl]piperidin-4-yl]-5-thia-1,8b-diazaacenaphthylene-4-carboxamide in ethanol (5 ml) was added, at room temperature, 2 ml (24 mmol.) of 12N hydrochloric acid. The mixture was stirred for one hour. The resulting crystalline precipitate was collected by filtration, followed by washing with ethanol and diethyl ether to afford the object compound (369.8 mg, 98%) as orange crystals.

Provenance & Evidence