Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Chlorophenol → 1-(4-Chlorophenoxy)acetone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Chlorophenol | HCID 4684 | — |
| 반응물 | Potassium Iodide | HCID 4875 | — |
| 반응물 | Chloroacetone | HCID 6571 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 1-(4-Chlorophenoxy)acetone | HCID 239874 | 97.5% |
반응 단계
4-Chlorophenol (10 g), chloroacetone (10.8 g), anhydrous potassium carbonate (12.9 g) and potassium iodide (1.3 g) were added to acetone (100 ml) and heated under reflux for 6 hours. The reaction mixture was filtered and the filtrate was concentrated to obtain 4-chlorophenoxyacetone (14 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06239077B1 |
| 출처 데이터셋 | uspto-grants-2001_05 |
| ORD ID | ord-cfa1616d65404d00b9f57ab28c931cd8 |
| 출처 메모 | uspto-grants-2001_05 |