HRID1978805

反应详情

EQUATION

反应方程式

HRID 1978805 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

4-Chlorophenol (10 g), chloroacetone (10.8 g), anhydrous potassium carbonate (12.9 g) and potassium iodide (1.3 g) were added to acetone (100 ml) and heated under reflux for 6 hours. The reaction mixture was filtered and the filtrate was concentrated to obtain 4-chlorophenoxyacetone (14 g).

WORKUP

后处理

  1. temperatureheated
  2. temperatureunder reflux for 6 hours
  3. filtrationThe reaction mixture was filtered
  4. concentrationthe filtrate was concentrated