HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53974740, compound → HCID 21202060, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53974740 | HCID 53974740 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21202060 | HCID 21202060 | — |
Reaction Steps
A mixture of tert-butyl 2-hydroxy-5-methoxycinnamate (27.5 g, 0.11 mol) and 10% Pd/C (2.6 g) in MeOH (350 mL) under H. pressure (45 psi) was shaken for 8 h and filtered. The filtrate was concentrated to to the titled compound (27 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06239138B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-6a046f730cc24ba5b948cdfd292a65d2 |
| Source note | uspto-grants-2001_05 |