HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 69663720, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69663720 | HCID 69663720 | — |
Reaction Steps
To the crude oxazolidinone amine residue 16a in DCM at room temperature was added pyridine (30 equivalents) and acetic anhydride (20 equivalents). The solution was stirred for 2 hrs and concentrated in vacuo. The oxazolidinone acetamide residue was purified by HPLC to provide pure oxazolidinone acetamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06239152B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-8d929a4cd8884d8e975fec773dc30976 |
| Source note | uspto-grants-2001_05 |