HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21201678, compound → HCID 21201619, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21201678 | HCID 21201678 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21201619 | HCID 21201619 | 108.2% |
Reaction Steps
N-(2-Nitrophenyl)-N-(2-cyanoethyl)-2-fluoroaniline (6.37 g) was dissolved in methanol (60 ml), 10% palladium carbon (0.60 g) was added, the mixture was stirred for 3 hours under hydrogen atmosphere. Palladium carbon was removed by filtration, the filtrate was concentrated under reduced pressure, to thereby obtain 6.17 g of the titled compound (Yield: 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06239131B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-35aff1df07194c92b56bd35db691e940 |
| Source note | uspto-grants-2001_05 |