1-Octanethiol → HCID 13362815, compound

Participants

Reaction Steps

In 1 ml of dimethylformamide there was mixed n-octyl (2-amino-5,6-dichloropyrazinyl)formate (100 mg; 0.312 mol), prepared in Step B above, and n-octyl thiol (150 mg; 0.936 mol), after which there was added triethylamine (70 mg; 0.624 mol), and the reaction mixture was stirred for 1 hour at room temperature. The reaction mixture was taken up in dichloromethane and passed through a silica gel column to give the title compound. Elemental Analysis:

Provenance & Evidence