HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 20439398, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 86739751 | HCID 86739751 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 20439398 | HCID 20439398 | 28.4% |
Reaction Steps
A solution of 4-methyl-5-[[3-[3-(1-piperidinylmethyl)phenoxy]propyl]amino]-4H-1,2,4-triazole-3-acetonitrile dioxalate (0.05 g) in 35% hydrochloric acid (1 ml) was heated at 40° C. for 3 h. The mixture was basified with sodium hydroxide and extracted with chloroform. Evaporation of the organic solution gave the title compound (0.01 g) as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04481199 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-186d1e8d016d42fe8f4e9c89e2c40319 |
| Source note | uspto-grants-1984_11 |