HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 20439483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 2-Chloro-6-methylnicotinic acid | HCID 121724 | — |
| Product | HCID 20439483 | HCID 20439483 | 50% |
Reaction Steps
2-Chloro-6-methyl nicotinic acid (3.5 g, 0.02 m) was refluxed with hydrazine hydrate (5 ml) and absolute alcohol (20 ml) for 5 hours. The solid was separated, washed with alcohol and crystallised from water to yield 50% of 2-hydrazino-6-methylnicotinic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04481268 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-3bdfdccd29824b53b0c634bf0c49270d |
| Source note | uspto-grants-1984_11 |