HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178484658, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178453625 | HCID 178453625 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178484658 | HCID 178484658 | — |
Reaction Steps
2,2-Dihydroxy-N,N-dimethylacetamide bis-[trans-4-(tert.-butyloxycarbonylaminomethyl)cyclohexanecarboxylate] (3 g) was dissolved in ethyl acetate (50 ml) and ethyl acetate containing hydrochloric acid (50 ml) was added. After 2 h the solvent was evaporated and the residue dissolved in methanol and ether was added. The precipitate formed (0.9 g) had a m.p. of 220° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04483867 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-b86a405953444d04bc518a8036b28638 |
| Source note | uspto-grants-1984_11 |