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HRID1979966

反应详情

EQUATION

反应方程式

HRID 1979966 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(C)(C)OC(=O)NC[C@H]1CC[C@H](C(=O)O)CC1.CC(C)(C)OC(=O)NC[C@H]1CC[C@H](C(=O)O)CC1.CN(C)C(=O)C(O)O
HCID178453625

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)C(=O)C(O)O.NC[C@H]1CC[C@H](C(=O)O)CC1.NC[C@H]1CC[C@H](C(=O)O)CC1
HCID178484658

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

2 次

PROCEDURE

实验过程

2,2-Dihydroxy-N,N-dimethylacetamide bis-[trans-4-(tert.-butyloxycarbonylaminomethyl)cyclohexanecarboxylate] (3 g) was dissolved in ethyl acetate (50 ml) and ethyl acetate containing hydrochloric acid (50 ml) was added. After 2 h the solvent was evaporated and the residue dissolved in methanol and ether was added. The precipitate formed (0.9 g) had a m.p. of 220° C.

WORKUP

后处理

  1. additionwas added
  2. customAfter 2 h the solvent was evaporated
  3. dissolutionthe residue dissolved in methanol
  4. additionether was added
  5. customThe precipitate formed (0.9 g)