HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 13363150, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Sc-36741 | HCID 175635 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 13363150 | HCID 13363150 | — |
Reaction Steps
A solution of 25.5 g (0.1 mole) of the title compound of Example 1 and 11 ml (ca. 0.11 mole) of acetic anhydride in 150 ml of pyridine was allowed to stand for about 16 hours at room temperature. Approximately half of the solution was separated and concentrated in vacuo to dryness and chromatographed on silica gel, giving the title compound, m.p. 181°-182°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04483987 |
| Source dataset | uspto-grants-1984_11 |
| ORD ID | ord-6c8fae4b4c4b4f4aa7d0c8e2b3756b74 |
| Source note | uspto-grants-1984_11 |