Pivaloyl chloride → HCID 13363153, compound

Participants

Reaction Steps

The title compound, m.p. 160°, was prepared by the method of Example 2 using 2.5 g (0.01 mole) of the product compound of Example 1 and 1.3 g (0.01 mole) of trimethylacetyl chloride, except that the reaction mixture was poured into 150 ml of water, giving a solid precipitate. Recrystallization from ethyl acetate/diethyl ether, rather than chromatography, afforded the title product.

Provenance & Evidence